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www.enargylab.can Helena, MT 817472 -0711 • Billings, MT 800 - 7354489 • Casper, WY 888 - 235 -1515 <br />Sim IM Gillette, WY 866 -686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888 -690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation Report Date: 10/18/13 <br />Project: Schwartz GW 9/24/13 S27176 & S27177 Work Order: 013090929 <br />Analyte Count Result Units RL ° /49EC Low Limit High Limit RPD RPDLimit Qual <br />Method: E365.1 Analytical Run: SUB- B212740 <br />Sample ID: ICV Initial Calibration Verification Standard 10/03/13 13:49 <br />Phosphorus, Total as P 0.229 mg /L 00050 92 90 110 <br />Method: E365.1 <br />Batch: B_74818 <br />Sample ID: MB -74818 <br />Method Blank <br />Run. SUB - 6212740 <br />10/03/13 13:51 <br />Phosphorus, Total as P <br />ND mg /L <br />0.004 <br />Sample ID: LCS -74818 <br />Laboratory Control Sample <br />Run: SUB - 6212740 <br />10/03/13 13:52 <br />Phosphorus, Total as P <br />0.186 mg /L <br />0.0050 <br />93 <br />90 <br />110 <br />Sample ID: 813092483- 002BMS <br />Sample Matrix Spike <br />Run: SUB- B212740 <br />10/03/13 14:06 <br />Phosphorus, Total as P <br />0.212 mg /L <br />0.0050 <br />98 <br />90 <br />110 <br />Sample ID: B13092483- 002BMSD <br />Sample Matrix Spike Duplicate <br />Run- SUB - 13212740 <br />10/03/13 14:07 <br />Phosphorus, Total as P <br />0.210 mg /L <br />0.0050 <br />97 <br />90 <br />110 0.9 <br />10 <br />Sample ID: B13092488- 003BMS <br />Sample Matrix Spike <br />Run: SUB- B212740 <br />10/03/13 14:24 <br />Phosphorus, Total as P <br />5.95 mg /L <br />0.050 <br />108 <br />90 <br />110 <br />Sample ID: B13092488- 003BMSD <br />Sample Matrix Spike Duplicate <br />Run: SUB- B212740 <br />10/03/13 14:25 <br />Phosphorus, Total as P <br />5.97 mg /L <br />0.050 <br />109 <br />90 <br />110 0.3 <br />10 <br />Method: E365.1 Analytical Run, SUB- B213411 <br />Sample ID: ICV Initial Calibration Verification Standard 10/16/13 09:30 <br />Phosphorus, Total as P 0.246 mg /L 0.0050 98 90 110 <br />Method: E365.1 <br />Sample ID: MB -75092 <br />Phosphorus, Total as P <br />Sample ID: LCS -75092 <br />Phosphorus, Total as P <br />Sample ID: 813100604- 010EMS <br />Phosphorus, Dissolved as P <br />Sample ID: 813100604- 010EMSD <br />Phosphorus, Dissolved as P <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />Method Blank <br />ND mg /L <br />Laboratory Control Sample <br />0.203 mg /L <br />Sample Matrix Spike <br />32.0 mg /L <br />Sample Matrix Spike Duplicate <br />32.2 mg /L <br />Batch: B 75092 <br />Run: SUB - 6213411 10/16/13 10:01 <br />0.004 <br />Run: SUB- B213411 10/16/13 10:02 <br />0.0050 101 90 110 <br />Run- SUB - 13213411 10/16/13 10:23 <br />0.25 104 90 110 <br />Run: SUB - 6213411 10/16/13 10:24 <br />0.25 105 90 110 <br />ND - Not detected at the reporting limit. <br />Page 17 of 23 <br />