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www.pm6ab.com ( Helena, MT 877- 472 -0711 • Billings, W B00- 735 -4489 • Casper, WY 88B- 235 -0515 <br />'t J Gillette, WY 866 -686 -7115 • Rapid City, SO 8BB -672 -1225 • College Station, TX 868- 690 -2218 <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation <br />Report Date: <br />09/05/13 <br />Project: Schwartz SW 8/6/13 <br />S27019 <br />Work Order: <br />C13080305 <br />[Analyte <br />Count Result <br />Units <br />RL <br />° /.REC <br />Low Limit <br />High Limit RPD <br />RPDLimit Qual <br />Method: E200.8 <br />Analytical Run: ICPMS2- C_130812A <br />Sample ID: ICV <br />11 Initial Calibration Verification Standard <br />08/12/13 21:11 <br />Aluminum <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Antimony <br />0.0529 <br />mg /L <br />0.0010 <br />106 <br />90 <br />110 <br />Arsenic <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Chromium <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Copper <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Lead <br />00497 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Manganese <br />0.0494 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Molybdenum <br />0.0500 <br />mg /L <br />0.0010 <br />100 <br />90 <br />110 <br />Thallium <br />0.0509 <br />mg /L <br />0.0010 <br />102 <br />90 <br />110 <br />Uranium <br />0.0496 <br />mg /L <br />0.00030 <br />99 <br />90 <br />110 <br />Zinc <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Method: E200.8 <br />Batch: 38624 <br />Sample ID: MB -38624 <br />11 Method Blank <br />Run: ICPMS2- C_130812A <br />08/12/13 21:30 <br />Aluminum <br />0.002 <br />mg /L <br />0.0005 <br />Antimony <br />0.0003 <br />mg /L <br />0.0002 <br />Arsenic <br />ND <br />mg /L <br />00003 <br />Chromium <br />0.002 <br />mg /L <br />0.0002 <br />Copper <br />0.0008 <br />mg /L <br />0.0004 <br />Lead <br />ND <br />mg /L <br />3E -05 <br />Manganese <br />ND <br />mg /L <br />7E -05 <br />Molybdenum <br />ND <br />mg /L <br />8E -05 <br />Thallium <br />ND <br />mg /L <br />0.0001 <br />Uranium <br />ND <br />mg /L <br />9E -06 <br />Zinc <br />0.0008 <br />mg /L <br />0.0005 <br />Sample ID: LCS3 -38624 <br />11 Laboratory Control <br />Sample <br />Run: ICPMS2- C_130812A <br />08/12/13 21:33 <br />Aluminum <br />2.45 <br />mg /L <br />0.030 <br />98 <br />85 <br />115 <br />Antimony <br />0.532 <br />mg /L <br />0.0010 <br />106 <br />85 <br />115 <br />Arsenic <br />0.476 <br />mg /L <br />0.0010 <br />95 <br />85 <br />115 <br />Chromium <br />0.489 <br />mg /L <br />0.0050 <br />97 <br />85 <br />115 <br />Copper <br />0.467 <br />mg /L <br />0.0050 <br />93 <br />85 <br />115 <br />Lead <br />0 510 <br />mg /L <br />0.0010 <br />102 <br />85 <br />115 <br />Manganese <br />2.41 <br />mg /L <br />0.0010 <br />97 <br />85 <br />115 <br />Molybdenum <br />0.526 <br />mg /L <br />0.0010 <br />105 <br />85 <br />115 <br />Thallium <br />0 506 <br />mg /L <br />0.00050 <br />101 <br />85 <br />115 <br />Uranium <br />0.551 <br />mg /L <br />0.00030 <br />110 <br />85 <br />115 <br />Zinc <br />0.468 <br />mg /L <br />0.010 <br />93 <br />85 <br />115 <br />Sample ID: C13080303 -001 DMS3 <br />11 Sample Matrix Spike <br />Run: ICPMS2- C_130812A <br />08/12/13 21:55 <br />Aluminum <br />2.42 <br />mg /L <br />0.030 <br />96 <br />70 <br />130 <br />Antimony <br />0.539 <br />mg /L <br />0.0010 <br />108 <br />70 <br />130 <br />Arsenic <br />0.465 <br />mg /L <br />0.0010 <br />93 <br />70 <br />130 <br />Chromium <br />0.479 <br />mg /L <br />0.0050 <br />96 <br />70 <br />130 <br />Copper <br />0.463 <br />mg /L <br />0.0050 <br />92 <br />70 <br />130 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />ND - <br />Not detected at the reporting limit. <br />MDC - Minimum detectable concentration <br />Page 12 of 25 <br />