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Analytical dzul'el reenanalytical.com p: 970247.4220 f: 970_.247.4227 75 Suttle Street Durango, CO 81303 <br />Laboratories <br />www. G reen A nalytica I. com <br />GCC Energy, LLC Project: Quarterly <br />6473 CR 120 Project Name / Number: King I and King II Reported: <br />Hesperus CO, 81326 Project Manager: Tom Bird 10/04/13 15:27 <br />General Chemistry - Quality Control <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch B309265 - General Prep - Wet Chem <br />Duplicate (B309265 -DUP2) <br />Source: 1309222 -03 <br />Prepared & Analyzed: 09/26/13 <br />PH <br />Reference (11309265 -SRMI) <br />7.96 pH Units <br />7.91 0.630 20 <br />Prepared & Analyzed: 09/26/13 <br />PH <br />Batch B309276 - General Prep - Wet Chem <br />8.45 pH Units <br />9.05 93.4 90 -110 <br />Blank (B309276 -BLKI) <br />Prepared & Analyzed: 09/27/13 <br />Sulfate <br />LCS (B309276 -BSI) <br />ND 10.0 mg/L <br />Prepared & Analyzed: 09/27/13 <br />Sulfate <br />LCS Dup (11309276 -181SDI) <br />46.0 10.0 mg/L <br />50.0 92.0 85 -115 <br />Prepared & Analyzed: 09/27/13 <br />Sulfate <br />48.0 10.0 mg/L <br />50.0 96.0 85 -115 4.26 20 <br />Batch B309287 - General Prep - Wet Chem <br />Blank (B309287 -BLKI) Prepared & Analyzed: 09/30/13 <br />Alkalinity, Total ND 10.0 mg/L <br />LCS (B309287 -BS1) Prepared & Analyzed: 09/30/13 <br />Alkalinity, Total 91.0 10.0 mg/L 100 91.0 85 -115 <br />LCS Dup (B309287 -BSD1) Prepared & Analyzed: 09/30/13 <br />Alkalinity, Total 95.0 10.0 mg/L 100 95.0 85 -115 4.30 20 <br />Green Analytical Laboratories The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirety. In no event <br />/I shall Green Analytical Laboratories be liable for incidental or consequential damages. <br />GALs liability, and clients exclusive remedy for any claim arising, shall be limited to the <br />amount paid by client for analyses. All claims, including those for negligence and any other <br />cause whatsoever, shall be deemed waived unless made in writing and received within <br />thirty days after completion of the applicable service. <br />Debbie Zufelt, Reports Manager <br />Page 7 of 12 <br />