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Analytical dzufelt@greenanalytical.com p 970.247.4220 f: 970.247.4227 75 Suttle Street Durango, CO 81303 <br />Laboratories <br />www.GreenAnalytical.com <br />GCC Energy, LLC Project: Quarterly <br />6473 CR 120 Project Name / Number: King I and King II Reported: <br />Hesperus CO, 81326 Project Manager: Tom Bird 10/04/13 15:27 <br />Dissolved Metals by ICP - Quality Control <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch B309278 - Dissolved Metals, E200.7/E200.8 <br />Blank (B309278 -BLKI) <br />Prepared: 09/30/13 Analyzed: 10/01/13 <br />Calcium <br />ND <br />1.00 <br />mg/L <br />Iron <br />ND <br />0.050 <br />mg/L <br />Magnesium <br />ND <br />1.00 <br />mg/L <br />Manganese <br />ND <br />0.005 <br />mg/L <br />Sodium <br />ND <br />1.00 <br />mg/L <br />LCS (B309278 -BSI) <br />Prepared: 09/30/13 Analyzed: 10/01/13 <br />Calcium <br />4.92 <br />1.00 <br />mg/L <br />5.00 98.5 85 -115 <br />Iron <br />5.03 <br />0.050 <br />mg/L <br />5.00 101 85 -115 <br />Magnesium <br />25.4 <br />1.00 <br />mg/L <br />25.0 101 85 -115 <br />Manganese <br />2.44 <br />0.005 <br />mg/L <br />2.50 97.5 85 -115 <br />Sodium <br />7.64 <br />1.00 <br />mg/L <br />8.10 94.4 85 -115 <br />LCS Dup (B309278 -BSD1) <br />Prepared: 09/30/13 Analyzed: 10/01/13 <br />Calcium <br />4.90 <br />1.00 <br />mg/L <br />5.00 98.1 85 -115 <br />0.425 <br />20 <br />Iron <br />5.01 <br />0.050 <br />mg/L <br />5.00 100 85 -115 <br />0.396 <br />20 <br />Magnesium <br />25.3 <br />1.00 <br />mg/L <br />25.0 101 85 -115 <br />0.327 <br />20 <br />Manganese <br />2.43 <br />0.005 <br />mg/L <br />2.50 97.2 85 -115 <br />0.320 <br />20 <br />Sodium <br />7.60 <br />1.00 <br />mg/L <br />8.10 93.9 85 -115 <br />0.536 <br />20 <br />Green Analytical Laboratories <br />--),s <br />t -U <br />Debbie Zufelt, Reports Manager <br />The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirety. In no event <br />shall Green Analytical Laboratories be liable for incidental or consequential damages. <br />GALS liability, and clients exclusive remedy for any claim arising, shall be limited to the <br />amount paid by client for analyses. All claims, including those for negligence and any other <br />cause whatsoever, shall be deemed waived unless made in writing and received within <br />thirty days after completion of the applicable service. <br />Page 9 of 12 <br />